Making Salts
Aim: To produce copper sulfate by reacting copper with an acid.
Equipment: Copper oxide powder, dilute (0.5 mol L-1)sulfuric acid,50 ml measuring cylinder, two 100 ml beakers, Bunsen burner, tripod, gauze mat, funnel, filter paper, Thermometer, Spatula, evaporating basin, stirring rod.
Method:
Method:
- Add 20 ml of sulfuric acid to a 100 ml beakers. heat the acid until it reaches 70℃. Turn off your Bunsen burner.
- Once heated, use a spatula to add pea-sized portions of copper oxide to the beaker. Stir the mixture for 30 seconds.
- Repeat step 2 until no more will dissolve. Allow the beaker to cool.
- Fold the filter paper and place in the fennel. Place the filter funnel into the seconds beaker.
- Make sure the beaker is cool enough to hold at the top. The contents should still be hot. you may need your teacher to complete this step.
- Gently swirl the contents of the beakers to mix, and then pour into the filter paper in the funnel. Allow to filter through.
- Rinse the beaker you used to heat the mixture previously, and place it back on top of your tripod filled with 50-60 ml of water.
- Place the evaporating basin on top of the beaker and carefully pour some of the solution from the beaker into the evaporating basin.
- Gently heat the beaker until solution in the evaporating basin has reduced by half.
- Leave the evaporating basin to cool. Once cool, move the evaporating basin to a warn place where it will not be disturbed(i.e a window-sill) and observe over the next few days. Blue copper sulfate crystals should form.
Copper oxide + Sulfuric acid → Copper fulfate + water.
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